Instructions for Submitting Samples

How to Submit Samples for Analysis at the Archaeometry Laboratory

The Archaeometry Laboratory analyzes, on average, over 5000 samples each year. Because we process such a high volume of samples, it is important that our collaborators provide specific information about their projects and their samples. Regardless of whether you are a first-time customer or a long-time colleague, the following instructions should be followed whenever you submit samples to our lab.

Additional instructions must be followed for the following types of samples:

In order to facilitate proper packaging and submission, we have prepared a checklist that can be downloaded and included with all samples.

Step 1: Contact Us

The first step in submitting samples to the lab for analysis is to contact us. Ideally, this should be done during the planning phase of your project. We may be able to offer suggestions regarding analytical method, number of samples, and type of samples required that will save you both time and money. By explaining your project goals, you will help us to better understand your project and better serve your needs.

Step 2: Assign Each Sample an Analytical ID (ANID)

We use a 6-digit identification system to uniquely identify every sample that we analyze. This number typically consists of three letters followed by three numbers (e.g., ABC001, ABC002, etc.). Before you begin assigning ANIDs to your samples, please contact us to either (1) obtain a discrete range of ANIDs, or (2) verify that your ANIDs have not been used for a previous project.

Do not write your ANIDs directly on your samples. Instead, write it (along with your last name and archaeological context) on a plastic zip-lock bag, and place your sample inside the bag. We prefer to use 6-mil White-Block reclosable bags, as these provide a stable writing surface for labeling samples. Alternatively, sample ANIDs can be written on a clean piece of paper or cardstock and inserted into the bag along with your samples.

If your samples are already in powder form, you may submit them in a screw- or snap-top vial (either glass or plastic). If you submit vials, please seal the caps with a piece of tape, and enclose the individual vials in small plastic bags. This will prevent cross-sample contamination should a vial, or vials, rupture during transit.

Assign your ANIDs consecutively and do not skip any numbers. This decreases the potential for confusion and errors, and makes it easier to track and inventory your samples.

Step 3: Prepare a Spreadsheet Inventory of your Samples

Upon receiving a project, the first thing we do is open the package and double check that all of the expected samples are present. Without an inventory of your samples, we have no way to ensure that we have received all of your samples. This also provides you with a final opportunity to verify that the information written on your sample bags is correct. A copy of this spreadsheet is useful because it saves us from having to retype the information once it arrives.

We use the Excel spreadsheet program, and we recommend that you provide either an Excel spreadsheet (*.XLS) or a dBase file (*.DBF). Spreadsheet inventories should be both emailed to the laboratory, and included on a 3.5" floppy disk or CD-Rom in your package.

Table of fields we require in your sample inventory:

To facilitate consistency in our database, we provide the following file templates that can be downloaded and modified for your project:

Once you have created this spreadsheet, print out a copy. You will need it for the next step.

Step 4: Prepare an Information Packet to Accompany your Samples

In archaeology, there is a maxim that "Context is Everything." This applies to all aspects of the archaeological project, including laboratory analysis. To best understand your project and your samples, we need to know as much about them as possible. Have other archaeologists analyzed similar materials in your region? If so, prepare a bibliography of these projects. Are you analyzing chert, obsidian, basalt, or another geological material? If so, provide us with photocopies of regional geological reports that discuss these materials.

The types of information we request with all projects are:

Step 5: Cover Letter

Prepare a cover letter that includes:

Step 6: Prepare your Parcel

Package your samples, computer disk, information packet, and cover letter into a single box. Envelopes are If your samples are fragile, remember to use packing material. If your samples are sharp-edged, such as rocks, you may want to double bag them. We strongly recommend that you send your samples in a durable box rather than an envelope. Our experiences have been that samples are often easily crushed (and therefore practically unusable) when shipped in an envelope, even thickly padded envelopes.

Step 7: Send your Parcel and Immediately Notify the Laboratory

Your parcel should be sent to the following address:

Attn: Dr. Michael D. Glascock
Archaeometry Laboratory
University of Missouri Research Reactor
1513 Research Park Drive
Columbia, MO 65211, USA

Shipments can be made through USPS, UPS, FedEx, and DHL.

Once you have sent your package, you must immediately contact us. We will need to know the following information:

We do not accept unexpected shipments of any kind.

If this information is not provided to us by the time the parcel arrives, the parcel will be rejected and returned to you.

Field Description
ANID 6-digit Identification number assigned by MURR
Alternate ID Your sample identification number. Examples include catalogue, inventory, or accession numbers.
Excavator Name of person or institution who oversaw excavation or collection of this material.
Source Person Name of person who is submitting this samples for analysis.
Affiliation Institution with which you are affiliated.
Region General region from which this sample comes from. Examples include: Southwest, Northeast, Middle East, Central Europe.
Country Country from which this sample originates.
State/Province State or province from which this sample originates.
County/District County or district from which this sample originates.
Subregion Subregion from which this sample originates. This generally refines an area to a specific geographic area such as a valley, rige, plain, etc.
Site Name Name of the site from which this sample originates.
Site Number Site classification number. For archaeological sites in the U.S., please use the Smithsonian numbering system. If these samples are from other countries, please use the proper national or regional numbering system. If there is no official numbering system, use a published reference and provide a citation in the 'Comments' field below.
Material Nature of the material being submitted. Examples include: Pottery, Clay, Temper (please indicate specific material), Soil, Daub, etc.
Ware General ware description (if submitting pottery). If your region of interest does not use the ware category, use the proper term for type of ceramic: Terra-cotta, Earthenware, Stoneware, China, or Porcelain.
Form Form of vessel from which the sherd originates (if known).
Paste General description of the ceramic paste. Generally this includes a statement about texture and/or color.
Major Temper The major tempering material.
Minor Temper Secondary tempering material.
Interior Decoration Description of any decorative elements on the inside of the sherd/vessel.
Exterior Decoration Description of any decorative elements on the outside of the sherd/vessel.
Culture Cultural group with which this material is affiliated.
Context General context of this sample. Examples can include unit numbers, loci, or some other site-specific area. Preferably these will be taken from excavation/survey records or publications.
Provenance Specific context of this sample. Examples can include excavation levels or some other notation that may be used to precisely identify where the artifact came from.
Period Phase, Horizon, or Period during which this material was believed to have been made. This should refine the designation in the field 'Culture.'
Date General dates ascribed to this material. Please give in calendrical years B.C/A.D.
Longitude Longitude of site. Please provide in WGS 1984.
Latitude Latitude of site. Please provide in WGS 1984.
UTM Zone Universal Transverse Mercator zone of site. If you use a system other than UTM, provide zone or datum here and give the name of the system in the 'Comments' field below.
Northing UTM (or other coordinate system) northing value.
Easting UTM (or other coordinate system) easting value.
Picture Picture or drawing of the sherd/vessel being submitted. If you do not have a picture of each individual sherd, you may provide a general picture or drawing for the ceramic type being analyzed. This field is optional, but recommended.
Comments Any additional comments or notes concerning this sample.
Table 1. Descriptions of the contextual data that must be submitted with samples of pottery, clay, and tempering materials. If you are unsure about what to include in contact the laboratory before sending your samples.
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Field Description
ANID 6-digit Identification number assigned by MURR
Alternate ID Your sample identification number. Examples include catalogue, inventory, or accession numbers.
Excavator Name of person or institution who oversaw excavation or collection of this material.
Source Person Name of person who is submitting this samples for analysis.
Affiliation Institution with which you are affiliated.
Region General region from which this sample comes from. Examples include: Southwest, Northeast, Middle East, Central Europe.
Country Country from which this sample originates.
State/Province State or province from which this sample originates.
County/District County or district from which this sample originates.
Subregion Subregion from which this sample originates. This generally refines an area to a specific geographic area such as a valley, rige, plain, etc.
Site Name Name of the site from which this sample originates.
Site Number Site classification number. For archaeological sites in the U.S., please use the Smithsonian numbering system. If these samples are from other countries, please use the proper national or regional numbering system. If there is no official numbering system, use a published reference and provide a citation in the 'Comments' field below.
Material Nature of the material being submitted. Examples include: Obsidian, Chert, Basalt, Rhyolite, etc.
Sample Type Use "Artifact" if this is an artifact, use "Source" if this is a piece from a geological source
Description Description of the piece being submitted. If it is an artifact, examples include: Bifacial tool, flake, core, blade, etc. If it is a piece representing a geological source, use descriptive terms such as Nodule/Cobble or Bedrock Sample.
Culture Use this field to list the cultural affiliation of the submitted piece. Only use this field if the piece you are submitting is an artifact.
Context General context of this sample. Examples can include unit numbers, loci, or some other site-specific area. Preferably these will be taken from excavation/survey records or publications.
Provenance Specific context of this sample. Examples can include excavation levels or some other notation that may be used to precisely identify where the artifact came from.
Period Phase, Horizon, or Period during which this material was believed to have been made. This should refine the designation in the field 'Culture.'
Date General dates ascribed to this material. Please give in calendrical years B.C/A.D.
Longitude Longitude of site. Please provide in WGS 1984.
Latitude Latitude of site. Please provide in WGS 1984.
UTM Zone Universal Transverse Mercator zone of site. If you use a system other than UTM, provide zone or datum here and give the name of the system in the 'Comments' field below.
Northing UTM (or other coordinate system) northing value.
Easting UTM (or other coordinate system) easting value.
Picture Picture or drawing of the artifact or source sample being submitted. If you do not have a picture of each individual piece, you may provide a general picture or drawing. This field is optional, but recommended.
Comments Any additional comments or notes concerning this sample.
Table 2. Contextual data that must be submitted with samples of obsidian, chert, and other geological materials. If you are unsure about what to include in contact the laboratory before sending your samples.
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Recent research reported by the Archaeometry Lab at MURR after June 2005 is based on support by the National Science Foundation under our current grant number 0504015.
Earlier research was supported by several NSF grants, including the following numbers: 8801707, 9102016, 9503035, 9802366, 9977237, 0102325, and 0405042.  Any opinions, findings and conclusions or recommendations expressed in this material are those of the author and do not necessarily reflect the views of the National Science Foundation.

Last Updated June 2, 2008
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