Instructions for Submitting Samples
How to Submit Samples for Analysis at the Archaeometry Laboratory
The Archaeometry Laboratory analyzes, on average, over 5000 samples each year. Because we process such a high volume of samples, it is important that our collaborators provide specific information about their projects and their samples. Regardless of whether you are a first-time customer or a long-time colleague, the following instructions should be followed whenever you submit samples to our lab.
Additional instructions must be followed for the following types of samples:
In order to facilitate proper packaging and submission, we have prepared a checklist that can be downloaded and included with all samples.
Step 1: Contact Us
The first step in submitting samples to the lab for analysis is to contact us. Ideally, this should be done during the planning phase of your project. We may be able to offer suggestions regarding analytical method, number of samples, and type of samples required that will save you both time and money. By explaining your project goals, you will help us to better understand your project and better serve your needs.
Step 2: Assign Each Sample an Analytical ID (ANID)
We use a 6-digit identification system to uniquely identify every sample that we analyze. This number typically consists of three letters followed by three numbers (e.g., ABC001, ABC002, etc.). Before you begin assigning ANIDs to your samples, please contact us to either (1) obtain a discrete range of ANIDs, or (2) verify that your ANIDs have not been used for a previous project.
Do not write your ANIDs directly on your samples. Instead, write it (along with your last name and archaeological context) on a plastic zip-lock bag, and place your sample inside the bag. We prefer to use 6-mil White-Block reclosable bags, as these provide a stable writing surface for labeling samples. Alternatively, sample ANIDs can be written on a clean piece of paper or cardstock and inserted into the bag along with your samples.
If your samples are already in powder form, you may submit them in a screw- or snap-top vial (either glass or plastic). If you submit vials, please seal the caps with a piece of tape, and enclose the individual vials in small plastic bags. This will prevent cross-sample contamination should a vial, or vials, rupture during transit.
Assign your ANIDs consecutively and do not skip any numbers. This decreases the potential for confusion and errors, and makes it easier to track and inventory your samples.
Step 3: Prepare a Spreadsheet Inventory of your Samples
Upon receiving a project, the first thing we do is open the package and double check that all of the expected samples are present. Without an inventory of your samples, we have no way to ensure that we have received all of your samples. This also provides you with a final opportunity to verify that the information written on your sample bags is correct. A copy of this spreadsheet is useful because it saves us from having to retype the information once it arrives.
We use the Excel spreadsheet program, and we recommend that you provide either an Excel spreadsheet (*.XLS) or a dBase file (*.DBF). Spreadsheet inventories should be both emailed to the laboratory, and included on a 3.5" floppy disk or CD-Rom in your package.
Table of fields we require in your sample inventory:
To facilitate consistency in our database, we provide the following file templates that can be downloaded and modified for your project:
Once you have created this spreadsheet, print out a copy. You will need it for the next step.
Step 4: Prepare an Information Packet to Accompany your Samples
In archaeology, there is a maxim that "Context is Everything." This applies to all aspects of the archaeological project, including laboratory analysis. To best understand your project and your samples, we need to know as much about them as possible. Have other archaeologists analyzed similar materials in your region? If so, prepare a bibliography of these projects. Are you analyzing chert, obsidian, basalt, or another geological material? If so, provide us with photocopies of regional geological reports that discuss these materials.
The types of information we request with all projects are:
- A map showing locations for each of the sites from which these samples were obtained. Please remember to include a scale, north arrow, and a common geographical landmark. If you are working in the U.S., please use a 7.5-minute topographic map of your project area, and provide the USGS quadrangle name. Visit the Mapping section on our Links page for suggestions on how you can obtain these.
- Geographic coordinates of the archaeological site/geological context from which your samples come. Coordinates should be given in Latitude/Longitude (WGS1984) and, if from the U.S.A., UTM Northing and Easting using NAD1983. If your samples are not from the U.S., please use WGS1984 Latitude/Longitude and specify what coordinate system or datum your UTM coordinates are in. Again, visit the Mapping section on our Links page for suggestions on how you can obtain these for your site.
- Background literature applicable to your project. Full bibliographic references will suffice for major journals, but please provide photocopies of CRM reports, local/regional journals, geological-service bulletins and maps, or unpublished material.
- The paper copy of the spreadsheet you created in Step 3.
Step 5: Cover Letter
Prepare a cover letter that includes:
- How many samples are being sent and their ANIDs.
- The technique by which these samples are to be analyzed (INAA, XRF, ICP-MS).
- Your email address, phone & fax numbers, and your mailing address.
- Your research questions and your goals for this project.
- The agreed-upon rate at which your samples will be processed and billed.
Step 6: Prepare your Parcel
Package your samples, computer disk, information packet, and cover letter into a single box. Envelopes are If your samples are fragile, remember to use packing material. If your samples are sharp-edged, such as rocks, you may want to double bag them. We strongly recommend that you send your samples in a durable box rather than an envelope. Our experiences have been that samples are often easily crushed (and therefore practically unusable) when shipped in an envelope, even thickly padded envelopes.
Step 7: Send your Parcel and Immediately Notify the Laboratory
Your parcel should be sent to the following address:
Attn: Dr. Michael D. Glascock
Archaeometry Laboratory
University of Missouri Research Reactor
1513 Research Park Drive
Columbia, MO 65211,
USA
Shipments can be made through USPS, UPS, FedEx, and DHL.
Once you have sent your package, you must immediately contact us. We will need to know the following information:
- Sender of package (this is usually you)
- Parcel-delivery service (e.g., UPS, USPS, FedEx, DHL, etc.)
- Tracking or Shipment Number
- Date of Expected Delivery
We do not accept unexpected shipments of any kind.
If this information is not provided to us by the time the parcel arrives, the parcel will be rejected and returned to you.
| Field |
Description |
| ANID |
6-digit Identification number assigned by MURR |
| Alternate ID |
Your sample identification number. Examples include catalogue, inventory,
or accession numbers. |
| Excavator |
Name of person or institution who oversaw excavation or collection of this
material. |
| Source Person |
Name of person who is submitting this samples for analysis. |
| Affiliation |
Institution with which you are affiliated. |
| Region |
General region from which this sample comes from. Examples include: Southwest,
Northeast, Middle East, Central Europe. |
| Country |
Country from which this sample originates. |
| State/Province |
State or province from which this sample originates. |
| County/District |
County or district from which this sample originates. |
| Subregion |
Subregion from which this sample originates. This generally refines an area
to a specific geographic area such as a valley, rige, plain, etc. |
| Site Name |
Name of the site from which this sample originates. |
| Site Number |
Site classification number. For archaeological sites in the U.S., please
use the Smithsonian numbering system. If these samples are from other countries,
please use the proper national or regional numbering system. If there is no
official numbering system, use a published reference and provide a citation
in the 'Comments' field below. |
| Material |
Nature of the material being submitted. Examples include: Pottery, Clay,
Temper (please indicate specific material), Soil, Daub, etc. |
| Ware |
General ware description (if submitting pottery). If your region of interest
does not use the ware category, use the proper term for type of ceramic: Terra-cotta,
Earthenware, Stoneware, China, or Porcelain. |
| Form |
Form of vessel from which the sherd originates (if known). |
| Paste |
General description of the ceramic paste. Generally this includes a statement
about texture and/or color. |
| Major Temper |
The major tempering material. |
| Minor Temper |
Secondary tempering material. |
| Interior Decoration |
Description of any decorative elements on the inside of the sherd/vessel. |
| Exterior Decoration |
Description of any decorative elements on the outside of the sherd/vessel. |
| Culture |
Cultural group with which this material is affiliated. |
| Context |
General context of this sample. Examples can include unit numbers, loci,
or some other site-specific area. Preferably these will be taken from excavation/survey
records or publications. |
| Provenance |
Specific context of this sample. Examples can include excavation levels
or some other notation that may be used to precisely identify where the artifact
came from. |
| Period |
Phase, Horizon, or Period during which this material was believed to have
been made. This should refine the designation in the field 'Culture.' |
| Date |
General dates ascribed to this material. Please give in calendrical years
B.C/A.D. |
| Longitude |
Longitude of site. Please provide in WGS 1984. |
| Latitude |
Latitude of site. Please provide in WGS 1984. |
| UTM Zone |
Universal Transverse Mercator zone of site. If you use a system other than
UTM, provide zone or datum here and give the name of the system in the 'Comments'
field below. |
| Northing |
UTM (or other coordinate system) northing value. |
| Easting |
UTM (or other coordinate system) easting value. |
| Picture |
Picture or drawing of the sherd/vessel being submitted. If you do not have
a picture of each individual sherd, you may provide a general picture or drawing
for the ceramic type being analyzed. This field is optional, but recommended. |
| Comments |
Any additional comments or notes concerning this sample. |
Table 1. Descriptions of the contextual
data that must be submitted with samples of pottery, clay, and tempering materials.
If you are unsure about what to include in contact the laboratory before sending your samples.
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| Field |
Description |
| ANID |
6-digit Identification number assigned by MURR |
| Alternate ID |
Your sample identification number. Examples include catalogue,
inventory, or accession numbers. |
| Excavator |
Name of person or institution who oversaw excavation or collection
of this material. |
| Source Person |
Name of person who is submitting this samples for analysis. |
| Affiliation |
Institution with which you are affiliated. |
| Region |
General region from which this sample comes from. Examples
include: Southwest, Northeast, Middle East, Central Europe. |
| Country |
Country from which this sample originates. |
| State/Province |
State or province from which this sample originates. |
| County/District |
County or district from which this sample originates. |
| Subregion |
Subregion from which this sample originates. This generally
refines an area to a specific geographic area such as a valley, rige, plain,
etc. |
| Site Name |
Name of the site from which this sample originates. |
| Site Number |
Site classification number. For archaeological sites in the
U.S., please use the Smithsonian numbering system. If these samples are
from other countries, please use the proper national or regional numbering
system. If there is no official numbering system, use a published reference
and provide a citation in the 'Comments' field below. |
| Material |
Nature of the material being submitted. Examples include:
Obsidian, Chert, Basalt, Rhyolite, etc. |
| Sample Type |
Use "Artifact" if this is an artifact, use "Source"
if this is a piece from a geological source |
| Description |
Description of the piece being submitted. If it is an artifact,
examples include: Bifacial tool, flake, core, blade, etc. If it is a piece
representing a geological source, use descriptive terms such as Nodule/Cobble
or Bedrock Sample. |
| Culture |
Use this field to list the cultural affiliation of the submitted
piece. Only use this field if the piece you are submitting is an artifact. |
| Context |
General context of this sample. Examples can include unit
numbers, loci, or some other site-specific area. Preferably these will be
taken from excavation/survey records or publications. |
| Provenance |
Specific context of this sample. Examples can include excavation
levels or some other notation that may be used to precisely identify where
the artifact came from. |
| Period |
Phase, Horizon, or Period during which this material was
believed to have been made. This should refine the designation in the field
'Culture.' |
| Date |
General dates ascribed to this material. Please give in calendrical
years B.C/A.D. |
| Longitude |
Longitude of site. Please provide in WGS 1984. |
| Latitude |
Latitude of site. Please provide in WGS 1984. |
| UTM Zone |
Universal Transverse Mercator zone of site. If you use a
system other than UTM, provide zone or datum here and give the name of the
system in the 'Comments' field below. |
| Northing |
UTM (or other coordinate system) northing value. |
| Easting |
UTM (or other coordinate system) easting value. |
| Picture |
Picture or drawing of the artifact or source sample being
submitted. If you do not have a picture of each individual piece, you may
provide a general picture or drawing. This field is optional, but recommended. |
| Comments |
Any additional comments or notes concerning this sample. |
Table 2. Contextual data that must be
submitted with samples of obsidian, chert, and other geological materials. If
you are unsure about what to include in contact the laboratory before sending
your samples.
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Recent research reported by the Archaeometry Lab at MURR after June 2005 is based on support by the National Science Foundation under our current grant number 0504015.
Earlier research was supported by several NSF grants, including the following numbers: 8801707, 9102016, 9503035, 9802366, 9977237, 0102325, and 0405042. Any opinions, findings and conclusions or recommendations expressed in this material are those of the author and do not necessarily reflect the views of the National Science Foundation.
Last Updated June 2, 2008
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University of Missouri–Columbia